Brookfield DV3T Rheometer Instrukcja Użytkownika Strona 111

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Brookeld Engineering Labs., Inc. Page 111 Manual No. M13-2100
BrookeldViscosityStandardsFluidsareaccurateto(+/-)1%oftheirstatedvalue.
Example:
CalculatetheacceptablerangeofviscosityusingDV3TRVwithRV-3Spindleat
2RPM;BrookeldStandardFluid12,500withaviscosityof12,257cPat25°C:
1) Calculatefullscaleviscosityrangeusingtheequation:
Full Scale Viscosity Range [cP] = TK
*
SMC
*
10,000
RPM
Where:
TK-1.0fromTable D-2
SMC=10fromTable D-1
Full Scale Viscosity Range
1
*
10
*
10,000
=
50,000 cP
2
Theviscosityisaccurateto(+/-)500cP(whichis1%of50,000)
2) Theviscositystandarduidis12,257cP.Itsaccuracyis(+/-)1%of12,257or
(+/-)122.57cP.
3) Totalallowableerroris(122.57+500)cP=(+/-)622.57cP.
4) Therefore,anyviscosityreadingbetween11,634.4and12,879.6cPindicatesthattheRheometer
isoperatingcorrectly.AnyreadingoutsidetheselimitsmayindicateaRheometerproblem.
ContacttheBrookeldtechnicalsalesdepartmentoryourlocalBrookelddealer/distributor
withtestresultstodeterminethenatureoftheproblem.
Example:
Calculate the acceptable accuracy for viscosity measurement using DV3TLV
withSC4-21spindleinSmallSampleAdapterat6,12,and30RPM.Brookeld
viscositystandarduid100cPshasanactualvalueof101.5cPat25ºC.
1) Calculate thefullscaleviscosity range eitherbyusing the SpindleRangeCoefcientin
AppendixBofMoreSolutionstoStickyProblemsorbyusingtheAutoRangebuttononyour
rheometer.
TheSpindleRangeCoefcientforthe21spindleonanLVTorqueinstrumentis4,688.
At6RPM,theFullScaleRange(FSR)viscosityis781cP.Allow+/-1%fortherheometer
and+/-1%fortheSmallSampleAdapter.Totalallowableaccuracyis:
+/-2%x781cP=+/-15.6cP
Asimilarcalculationat12RPMgivesFSR=391cP:+/-2%x391cP=+/-7.8cP
Asimilarcalculationat30RPMgivesFSR=156cP:+/-2%x156cP=+/-3.1cP
2) TheViscosityStandardFluidis101.5cP.Itsaccuracyis:
+/-1%x101.5cP=+/-1.015cPorroughly+/-1.0cPforfurthercalculations.
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